Methyl N-phenyl carbamate synthesis from aniline and methyl formate: carbon recycling to chemical products.

Mohammad S Yalfani, Giulio Lolli, Thomas E Müller, Aurel Wolf, Leslaw Mleczko
Author Information
  1. Mohammad S Yalfani: CAT Catalytic Center, RWTH Aachen University, Worringerweg 2, 52074 Aachen (Germany).

Abstract

Methyl N-phenyl carbamate was synthesized from aniline by using methyl formate as a green and efficient carbonylating agent. High yields were obtained at milder reaction conditions compared to the conventional CO/CH3 OH route. Studies on the reaction sequence led to suggest an alternative and more efficient route to the carbamate via formanilide as intermediate.

Keywords

MeSH Term

Aniline Compounds
Carbamates
Carbon
Chemistry Techniques, Synthetic
Formic Acid Esters
Green Chemistry Technology
Oxidation-Reduction
Recycling

Chemicals

Aniline Compounds
Carbamates
Formic Acid Esters
methyl formate
Carbon
aniline

Word Cloud

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