[Structure analysis of benzoic medicines by near infrared and two dimensional correlation spectroscopy].

Hao Liu, Bing-ren Xiang, Ling-bo Qu, Jian-ping Xu
Author Information
  1. Hao Liu: Department of Pharmacy, Guangdong Chemical Engineering Pharmaceutics College, Guangzhou 510520, China.

Abstract

The structure analysis of benzoic medicines by Fourier transform near infrared spectroscopy and generalized two dimensional correlation spectroscopy was performed. Three kinds of medicines showed unconspicuous changes in one-dimensional near infrared spectra, while the two dimensional correlation spectra showed high resolution, and were more explicable. By the comparison and analysis of raw near infrared spectra and 2D-correlation spectra, the near infrared absorption peaks of benzoic acid medicines were assigned, and their structure characteristics were analyzed, the results affirmed the six-membered ring intramolecular hydrogen bond especially. The study is helpful to the in-depth understanding of benzoic medicines, and provides information for the future study and utilization of benzoic medicines.

MeSH Term

Benzoates
Hydrogen Bonding
Magnetic Resonance Spectroscopy
Molecular Structure
Spectroscopy, Fourier Transform Infrared
Spectroscopy, Near-Infrared

Chemicals

Benzoates

Word Cloud

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